Food Adulteration and Its Detection. Jesse P. Battershall

Food Adulteration and Its Detection - Jesse P. Battershall


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      PLATE II.

      TEA LEAVES.

      The portion of ash insoluble in acids consisted of silica, clay, and soapstone, indicating that the ash of tea dust is largely composed of the mineral substances employed for “facing” purposes.

      The characteristics of the ash of unspent tea are the presence of manganic oxide, the large proportion of potassium salts present, and the solubility of the ash in water. The amount of ash in genuine tea ranges from five to six per cent. In the absence of exhausted leaves, it has been found that the finer sorts of tea afford a smaller proportion of ash than the inferior grades. It will be noticed that spent tea ash exhibits a marked increase in the proportion of insoluble compounds (silica, alumina, and ferric oxide), as well as a total absence of potassium salts.

      The presence of foreign leaves, and, in some instances, of mineral adulterants in tea is best detected by means of a microscopical examination of the suspected sample. The genuine tea-leaf is characterised by its peculiar serrations and venations. Its border exhibits serrations which stop a little short of the stalk, while the venations extend from the central rib, nearly parallel to one another, but turn just before reaching the border of the leaf.

      Plate I. (Frontispiece) is a photogravure of a twig of the tea plant, in possession of the author. The leaves are of natural size, but the majority are of a greater maturity than those used in the preparation of tea, which more resemble in size the few upper leaves.

      Plate III. exhibits some of these leaves, two genuine Japan tea-leaves being included for purpose of comparison. The leaves represented in this plate are: 1, beech; 2, hawthorn; 3, rose; 4, Japan tea; 5, willow; 6, te-mo-ki; 7, elm; 8, wisteria; 9, poplar. From very recent reports of the American consuls in Japan and China, it would appear that the addition of foreign leaves to tea is at present but seldom resorted to, and this accords with the author’s experience in the testing of the teas imported into this country.

      In 1884, the Japanese Government made it a criminal offence to adulterate tea, and instituted “tea guilds,” which are governed by very stringent laws, and of which most dealers of repute are members. The facing of tea does not appear, however, to have been considered an adulteration, its continued practice being justified by the plea that otherwise Japan teas would not suit the taste of American consumers.

      PLATE III.

      TEA AND OTHER LEAVES.

      In the microscopic examination of tea, the sample should be moistened with hot water and spread out on a glass plate, and then submitted to a careful inspection, especial attention being directed to the general outline of the leaf and its serrations and venations. The presence of exhausted tea-leaves may often be detected by their soft texture and generally disintegrated appearance. If a considerable quantity of the tea be placed in a long glass cylinder and agitated with cold water, the colouring and other abnormal substances frequently become detached, and either rise to the surface of the liquid as a sort of scum, or fall to the bottom as a sediment. In this way Prussian blue, indigo, soapstone, gypsum, sand, and turmeric can often be separated, and subsequently recognised by their characteristic appearance under the microscope. The separated substances should also be subjected to a chemical examination. Prussian blue is detected by heating with a solution of sodium hydroxide, filtering, acidulating the filtrate with acetic acid, and then adding ferric chloride, when, in its presence, a blue colour will be produced. Indigo is best recognised by the microscopic examination. It is not decolorised by caustic alkali, but it dissolves in sulphuric acid to a blue liquid. Soapstone, gypsum, sand, and metallic iron, are identified by means of the usual chemical reactions. A compound very aptly termed “Lie-tea,” is sometimes met with. It forms little pellets, consisting of tea-dust mixed with foreign leaves, sand, etc., and held together by means of gum or starch. This falls to powder if treated with boiling water. In the presence of catechu, the tea infusion usually assumes a muddy appearance upon standing. In case iron salts have been employed to deepen the colour of the infusion, they can be detected by treating the ground tea-leaves with acetic acid, and testing the filtered solution with potassium ferrocyanide. Tea should not turn black upon immersion in hydrosulphuric acid water, nor should it impart a blue colour to ammonia water. The infusion should be amber-coloured, and not become reddened by the addition of an acid.

      The United States Tea Adulteration Act was passed by Congress in 1883. The enactment of this law was largely due to the exertions of prominent tea merchants, whose business interests were seriously affected by the sale (principally in trade auctions) of the debased or spurious article. It is stated in the official report of the United States Tea Examiner at New York City, that from March 1883 to December of the same year, 856,281 packages (about four millions of pounds) of tea were inspected, of which 7000 packages (325,000 pounds) were rejected as unfit for consumption. Since the enforcement in New York City of the Tea Adulteration Act, nearly 2000 samples of tea have been chemically tested under the direction of the author. The proportion grossly adulterated has been a little over nine per cent. But this does not apply to the total amount imported, since only those samples which were somewhat suspicious in appearance were submitted for analysis. As the result of the past two years’ experience in the chemical examination of tea, the prevailing adulterations were found to be of two kinds—the admixture of spent tea-leaves, and the application to the tea of a facing preparation. A natural green tea possesses a dull hue, and is but seldom met with in the trade; some Moyunes and uncoloured Japans (which latter, properly speaking, is not a green tea) being almost the only varieties not exhibiting the bright metallic lustre due to the facing process. The addition of foreign leaves was detected only in a few instances; the presence of sand and gravel occurred far more frequently. Apropos of the practical utility of Governmental sanitary legislation, it can be stated that, since the enforcement of the Adulteration Act, the tea imported into the city of New York has very perceptibly improved in quality.

      Attempts in tea culture are being made in the United States of Columbia, S.A. A specimen of the prepared plant received by the writer, differed greatly in appearance from the Chinese and Japanese products. The leaves, which had not been rolled but were quite flat, possessed a light pea-green colour and a fine but rather faint aroma. An examination indicated that the tea, although very delicate in quality, was seriously deficient in body.

      The analysis showed:—

Per cent.
Moisture 6·70
Total ash 4·82
Ash soluble in water 1·62
Ash insoluble in water 3·20
Ash insoluble in acid 0·16
Extract 27·40
Tannic acid 4·31
Theine 0·66
Insoluble leaf 65·90

      The


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